Graduation Semester and Year

Summer 2024

Document Type

Dissertation

Degree Name

Doctor of Philosophy in Biomedical Engineering

Department

Bioengineering

First Advisor

Dr. Justyn Jaworski

Second Advisor

Dr. Kytai T. Nguyen

Third Advisor

Dr. Cesar Torres

Abstract

Polydiacetylene based materials have been used for a variety of liquid phase sensing applications. There remains a need for low cost, easy-to-read gas phase sensors for continuous monitoring of physiological parameters and environmental hazards at work or at home. Such sensors could have applications in everyday life, for example as point-of-care or at home testing devices to enable early detection of disease to reduce healthcare costs. Making accessible and non-invasive technologies for monitoring of health and health risks provides individuals with the ability to be proactive in regard to their health and safety. In other examples, environmental monitoring systems could be used to detect harmful pollutants through direct detection of compounds in the air or water supply. Here I present a new sensing technique in which diacetylene amphiphile containing monomers with unique head group chemistry containing dipicolylamine were used in the detection of lead in liquid phase. The exclusive selectivity of this sensor to lead and the high sensitivity revealed a color change from blue to red upon detection of lead ions in water. In another application, iron containing diacetylene formulations were developed to form the first spray on sensor for the detection of H2O2 vapors in the air. These formulations enabled the catalysis of H2O2 to hydroxyl radicals that served as an initiator in the polymerization of the diacetylene containing amphiphile, causing a white to blue color transition. With this affordable sensing approach, new capabilities open up for the utilization of spray-on sensors for the detection of chemical targets or physical stimuli without the need for training or understanding of complex analytical systems.

Keywords

Diacetylene-based, amphiphile, spray-on, sensor, environmental monitoring, polymer, Pentacosadiynoic acid, self-assembly, dipicolylamine, hydrogen peroxide vapor

Disciplines

Biomedical Engineering and Bioengineering | Polymer and Organic Materials

License

Creative Commons Attribution 4.0 International License
This work is licensed under a Creative Commons Attribution 4.0 International License.

Available for download on Sunday, February 09, 2025

Share

COinS